问题：求助,物化性质及相关资料
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时间：2007-07-26 07:43:10 编辑加入/取消收藏订制/取消短消息举报该贴

那位仁兄有相关2,4-二甲氧基乙酰苯胺的物化性质及相关的合成资料,如有请发至邮箱lwz5236@163.com

回复人：zhouxr,▲ (从事有机合成的教学和科研) 时间：2007-07-27 19:44:02 编辑

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CAS Registry Number: 23042-75-3
Molecular Formula: C10H13NO3
Molecular Weight: 195.218
Accurate Mass: 195.089544
Percentage Composition: C 61.53%; H 6.71%; N 7.17%; O 24.59%
Physical Description: Cryst. (Me2CO aq.)
Melting Point: Mp 117

References:
Aldrich Library of FT-IR Spectra, 1st edn., 1985, 1, 1225D; 1226A, (ir)
Aldrich Library of 13C and 1H FT NMR Spectra, 1992, 2, 513A, (nmr)
Aldrich Library of FT-IR Spectra: Vapor Phase, 1989, 3, 1145B, (ir)
Bechhold, J., Ber., 1889, 22, 2374, (synth)
Henrich, F. et al., Ber., 1902, 35, 4195, (synth)
Heidelberger, M. et al., J.A.C.S., 1919, 41, 1450, (synth)
Barton, D.H.R. et al., J.C.S., 1945, 436, (synth, deriv)
Dey, B.B. et al., J. Sci. Ind. Res., Sect. B, 1951, 10, 175; CA, 48, 58176, (synth, deriv)
Loudon, J.D. et al., J.C.S., 1955, 739, (deriv)
Lantz, R.L. et al., Bull. Soc. Chim. Fr., 1961, 2402, (synth)
Hill, J. et al., J.C.S., 1964, 3709, (synth, deriv)
Collins, R.F. et al., J.C.S.(C), 1966, 366, (synth)
Sunkel, J. et al., Ber. Bunsen-Ges. Phys. Chem., 1969, 73, 203, (uv)
Grant, D.F. et al., Z. Kristallogr., Kristallgeom., Kristallphys., Kristallchem., 1970, 132, 385, (cryst struct)
Catto, A. et al., Tet. Lett., 1973, 2723, (synth, ir, deriv)
Richey, J.D. et al., Agric. Biol. Chem., 1975, 39, 683, (synth, ir, deriv)
Nachman, R.J., J. Het. Chem., 1982, 19, 1545, (synth, ms, pmr, deriv)
Messer, C. et al., CA, 1999, 131, 71415y, (2,4-Dimethoxyaniline, isol)
Findlay, J.A. et al., Can. J. Chem., 2003, 81, 284-292, (4-Hydroxy-2-methoxyacetanilide, isol, pmr, cmr)

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